About TCAW - Subscription Info
February 2001
Vol. 10, No. 02, p. 48.
Focus: Separation Sciences

FEATURE

“Committeeing” to Calibrate

Figure 4
Part of the template form to document the calibration of the autosampler.

HPLC Calibration Template

13. AUTOSAMPLER CALIBRATION

Autosampler manufacturer:_____________________________

____________________________________________________

Autosampler ID: ______________________________________

Flow rate: 1.0 mL/min Wavelength: 258 nm

Next calibration due:___________________________________

13.1. Reproducibility of Autosampler

RSD of peak areas:_________%________ (Specification: 0.5%)

Millennium result ID:___________________________________

Reproducibility: __ Pass __ Fail

13.2. Linearity of Autosampler

Correlation coefficient (R):__________(Specification: >0.999)

Millennium result ID: ____________Linearity: __ Pass __ Fail

13.3. Carryover of Autosampler

Carryover (%):____________________ (Specification: <1.0%)

Millennium result ID: ____________Carryover: __ Pass __ Fail

Back to: "Committeeing" to Calibrate HPLC